Noncovalent derivatives of hydroquinone: bis-(N,N-dialkyl)bicyclo[2.2.2]octane-1,4-dicarboxamide complexes

Bruce M Foxman; Donna J Guarrera; Ramdas Pai; Carlos Tassa; John C Warner

doi:10.1016/S1463-0184(99)00007-6

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Noncovalent derivatives of hydroquinone: bis-(N,N-dialkyl)bicyclo[2.2.2]octane-1,4-dicarboxamide complexes

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Noncovalent derivatives of hydroquinone: bis-(N,N-dialkyl)bicyclo[2.2.2]octane-1,4-dicarboxamide complexes

Bruce M Foxman, Donna J Guarrera, Ramdas Pai, Carlos Tassa and John C Warner

Crystal engineering, Vol.2(1), pp.55-64

09/01/1999

DOI: https://doi.org/10.1016/S1463-0184(99)00007-6

Abstract

crystal structure

phase transitions

thermodynamic properties

organic compounds

Crystal Growth

The solid state phase behavior of hydroquinone with bis-(N,N-diethyl)bicyclo[2.2.2]octane-1,4-dicarboxamide ( ) and with bis-(N,N-dimethyl)bicyclo[2.2.2]octane-1,4-dicarboxamide ( ) has been investigated. A 1:1 complex, , exists with hydroquinone and the diethyl derivative . A 1:2 complex, , and a 2:1 complex, , is formed with hydroquinone and the dimethyl derivative, . X-ray structure determinations of these cocrystals have been performed and the role of the alkyl side chains in the crystal packing is discussed.

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Title: Noncovalent derivatives of hydroquinone: bis-(N,N-dialkyl)bicyclo[2.2.2]octane-1,4-dicarboxamide complexes
Creators: Bruce M Foxman - Department of Chemistry, Brandeis University, Waltham, MA 02454, USA
Donna J Guarrera - Polaroid Corporation, Media Systems Research Laboratories, Cambridge, MA 02139, USA
Ramdas Pai - Polaroid Corporation, Media Systems Research Laboratories, Cambridge, MA 02139, USA
Carlos Tassa - Department of Chemistry, University of Massachusetts Boston, 100 Morrissey Blvd., Boston, MA 02125, USA
John C Warner - Department of Chemistry, University of Massachusetts Boston, 100 Morrissey Blvd., Boston, MA 02125, USA
Publication Details: Crystal engineering, Vol.2(1), pp.55-64
Publisher: Elsevier Ltd
Identifiers: 9923989589401921
Academic Unit: Department of Chemistry
Language: English
Resource Type: Journal article

Noncovalent derivatives of hydroquinone: bis-(N,N-dialkyl)bicyclo[2.2.2]octane-1,4-dicarboxamide complexes

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