Logo image
Home Academic units
Sign in
Organocatalytic Asymmetric Mannich Reaction of Malonates with Imines
Journal article   Peer reviewed

Organocatalytic Asymmetric Mannich Reaction of Malonates with Imines

J Song, Y Wang and L Deng
Synfacts, Vol.2006(6), pp.612-612
06/2006

Abstract

Here the authors report a highly enantioselective Mannich reaction of N-Boc imines with malonates and β-keto esters. Bifunctional cinchona alkaloid based catalyst 1 bearing a 6′-thiourea functionality was found to be effective for the reaction. In the presence of 20 mol% of the catalyst, good yields (81-99%) and high enantio­selectivities (96-99%) are obtained for different aryl imines. One equivalent of the catalyst was required in order to obtain high enantioselectivities with alkyl imines.

Metrics

26 Record Views

Details