Rapid three-dimensional MAS NMR spectroscopy at critical sensitivity

Yoh Matsuki; Matthew T Eddy; Robert G Griffin; Judith Herzfeld

doi:10.1002/anie.201003329

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Rapid three-dimensional MAS NMR spectroscopy at critical sensitivity

Journal article

Peer reviewed

Rapid three-dimensional MAS NMR spectroscopy at critical sensitivity

Yoh Matsuki, Matthew T Eddy, Robert G Griffin and Judith Herzfeld

Angewandte Chemie (International ed.), Vol.49(48), pp.9215-9218

10/18/2010

DOI: https://doi.org/10.1002/anie.201003329

PMCID: PMC3495158

PMID: 20957710

Abstract

Non-uniform sampling

Solid-state NMR

SIFT

Protein NMR

Rapid Acquisition

Sensitive SIFTing: Multidimensional non-uniform sampling (NUS) NMR spectroscopy is extended to the severely sensitivity-limited regime typical of MAS NMR of biomacromolecules by the use of spectroscopy by the integration of frequency and time domain information (SIFT). A three-dimensional MAS NMR experiment is expedited (here 3.4-fold) without losing sensitivity or resolution.

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Title: Rapid three-dimensional MAS NMR spectroscopy at critical sensitivity
Creators: Yoh Matsuki - Department of Chemistry, Brandeis University, Waltham MA 02454 (USA), Fax: (+1) 781 736 2538. Department of Chemistry and Francis Bitter Magnet Laboratory, Massachusetts Institute of Technology, Cambridge MA 02139 (USA)
Matthew T Eddy - Department of Chemistry and Francis Bitter Magnet Laboratory, Massachusetts Institute of Technology, Cambridge MA 02139 (USA)
Robert G Griffin - Department of Chemistry and Francis Bitter Magnet Laboratory, Massachusetts Institute of Technology, Cambridge MA 02139 (USA)
Judith Herzfeld - Department of Chemistry, Brandeis University, Waltham MA 02454 (USA), Fax: (+1) 781 736 2538
Publication Details: Angewandte Chemie (International ed.), Vol.49(48), pp.9215-9218
Identifiers: 9923972931601921
Academic Unit: Department of Chemistry
Language: English
Resource Type: Journal article

Rapid three-dimensional MAS NMR spectroscopy at critical sensitivity

Abstract

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